Related Compounds A and B in Drug Product,” and “Validation of Analytical Test Procedures,” SOP Number ABC-1243 rev4 dated 1 April 2002. III. EXPERIMENTAL A. Reagents Sodium acetate, Tisher, HPLC grade Glacial acetic acid, Tisher, HPLC grade Acetonitrile, Tisher, Suptima grade THF, Tisher, Suptima grade Water, in-house deionized water B